陈海燕
,
曾键波
,
谢羽
,
路美秀
,
牛艳
,
李霞
材料工程
doi:10.11868/j.issn.1001-4381.2015.11.010
为保证Sn-Sb-Cu-Ni合金及焊点在低温环境下使用可靠性,将SnSb 4.5CuNi合金焊料和焊点在25,-10,-20,-60℃恒温环境中进行储存565天后,考察了不同温度下SnSb 4.5CuNi合金微观组织形貌、物相、密度、电导率、抗拉强度和塑性的变化,通过纳米压痕法测量SnSb 4.5CuNi/Cu焊点界面过渡层Cu6Sn5金属间化合物(IMC)的硬度和弹性模量,对焊接接头进行抗拉强度、剪切强度和低周疲劳测试.结果表明:合金主要由SbSn和β-Sn组成,低温处理565天后合金组织形貌逐渐转变为树枝状组织,焊料合金的密度和电导率均随温度降低而升高,表明经低温储存后合金没有发生灰锡转变,但脆性SbSn相析出量的增多和枝晶组织致使铸态合金的拉伸强度降低,增加了合金脆断风险;随着温度的下降,焊接界面IMC层的弹性模量和硬度增大,焊件拉伸破坏模式从焊料内部转为IMC层,断口越趋平整,焊件的抗拉强度、抗剪强度下降,呈现了低温脆性断裂的倾向.
关键词:
无铅焊料
,
显微组织
,
低温脆性
,
纳米压痕测试
,
低周疲劳
HUANG Zheng Institute of Physics
,
Academia Sinica
,
Beijing
,
ChinaYAO Mei Harbin Institute of Technology
,
Harbin
,
China Institute of Physics
,
Academia Sinica
,
Beijing 100080
,
China
金属学报(英文版)
On the basis of analysis of low carbon steel fracture macro-features and micro-processes at low temperature,the definition was given of the characteristic transition temperature of brittleness,T_(pm),and its physical meaning was expounded.Discussion was carried out of phys- ical characteristic of variation at T_(pm) in respect of the fracture toughness and property of crack arrest.In addition,research was made on the application of T_(pm),which can give infor- mation about the transition of the fracture toughness,the property of crack arrest and critical crack size,to estimation the brittleness of low carbon steel at low temperatures.
关键词:
low carbon steel
,
null
,
null
,
null
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